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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 607325Generated: November 2, 2026

HCID 66808620, compound → HCID 57667805, compound

https://huagongshe.com/reaction/607325

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 66808620HCID 66808620—
ReactantHCID 178418361HCID 178418361—
CatalystPalladiumHCID 23938—
SolventEthanolHCID 702—
ProductHCID 57667805HCID 57667805—

Reaction Steps

A mixture of the product from Example 241A (0.166 g, 0.694 mmol) and 10% palladium on charcoal (18.4 mg, 0.025 eq), in ethanol (10 mL) was stirred under one atmosphere of hydrogen for 16 hours. The reaction mixture was then filtered through Celite and the solvent evaporated under reduced pressure to provide the title compound as a slightly red oil (0.141 g, 96% yield).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07915411B2
Source datasetuspto-grants-2011_03
ORD IDord-46a00a0a139840c593a7a730ab3a2cdb
Source noteuspto-grants-2011_03