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HRID608077

反应详情

EQUATION

反应方程式

HRID 608077 的结构方程式

REACTANTS

反应物

2
结构：CN(C)c1ccc(B2OC(C)(C)C(C)(C)O2)cc1
HCID2758659

N,N-Dimethyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)aniline

C14H22BNO2

结构：CC(=O)NC(C)(C)[C@@H]1CC2(CCN(C(=O)OC(C)(C)C)CC2)c2cc(Cl)c(C)cc21
HCID24805585

未命名化合物

PRODUCTS

生成物

3
结构：c1ccc(-c2ccccc2)cc1
HCID7095

Biphenyl

C12H10

结构：CC(=O)NC(C)(C)[C@@H]1CC2(CCN(C(=O)OC(C)(C)C)CC2)c2cc(Cl)c(C)cc21
HCID24805585

未命名化合物

结构：CC(=O)NC(C)(C)[C@@H]1CC2(CCN(C(=O)OC(C)(C)C)CC2)c2cc(-c3ccc(N(C)C)cc3)c(C)cc21
HCID178474760

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

4
结构：CC(C)Oc1cccc(OC(C)C)c1-c1ccccc1[PH](C1CCCCC1)(C1CCCCC1)[Pd]1(OS(C)(=O)=O)Nc2ccccc2-c2ccccc21
催化剂HCID178458464

未命名化合物

结构：CS(C)=O
溶剂HCID679

Dimethyl sulfoxide

C2H6OS

结构：O
溶剂HCID962

Water

H2O

结构：O=P(O)(O)O.[K]
其他HCID16218557

未命名化合物

WORKUP

后处理

  1. additionAfter 22 hours the crude reactions were diluted with 3 x 1 uL 0.5 M AcOH in DMSO (containing PhPh as an internal standard). The reactions were mixed after each dispense operation.
  2. aliquotMosquito(R) was used to transfer 1 uL of each quenched reaction from the 1,536-well reaction plate to 384-well analytical plates containing 60 uL DMSO for analysis.