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HRID608095

反应详情

EQUATION

反应方程式

HRID 608095 的结构方程式

REACTANTS

反应物

2
结构：O=C(NC1CCCC1)c1ccc(B(O)O)cc1
HCID2773358

[4-(Cyclopentylcarbamoyl)phenyl]boronic acid

C12H16BNO3

结构：CC(=O)NC(C)(C)[C@@H]1CC2(CCN(C(=O)OC(C)(C)C)CC2)c2cc(Cl)c(C)cc21
HCID24805585

未命名化合物

PRODUCTS

生成物

3
结构：c1ccc(-c2ccccc2)cc1
HCID7095

Biphenyl

C12H10

结构：CC(=O)NC(C)(C)[C@@H]1CC2(CCN(C(=O)OC(C)(C)C)CC2)c2cc(Cl)c(C)cc21
HCID24805585

未命名化合物

结构：CC(=O)NC(C)(C)[C@@H]1CC2(CCN(C(=O)OC(C)(C)C)CC2)c2cc(-c3ccc(C(=O)NC4CCCC4)cc3)c(C)cc21
HCID178474758

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

4
结构：CC(C)c1cc(C(C)C)c(-c2ccccc2[PH](C2CCCCC2)(C2CCCCC2)[Pd]2(OS(C)(=O)=O)Nc3ccccc3-c3ccccc32)c(C(C)C)c1
催化剂HCID178439024

未命名化合物

结构：CS(C)=O
溶剂HCID679

Dimethyl sulfoxide

C2H6OS

结构：O
溶剂HCID962

Water

H2O

结构：O=P(O)(O)O.[K]
其他HCID16218557

未命名化合物

WORKUP

后处理

  1. additionAfter 22 hours the crude reactions were diluted with 3 x 1 uL 0.5 M AcOH in DMSO (containing PhPh as an internal standard). The reactions were mixed after each dispense operation.
  2. aliquotMosquito(R) was used to transfer 1 uL of each quenched reaction from the 1,536-well reaction plate to 384-well analytical plates containing 60 uL DMSO for analysis.