HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,5-Dimethylisoxazole-4-boronic acid pinacol ester → 2-(3,5-Dimethyl-1,2-oxazol-4-yl)-5-methylbenzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,5-Dimethylisoxazole-4-boronic acid pinacol ester | HCID 2758656 | — |
| Reactant | 5-Methyl-2-(1-methyl-1H-pyrazol-4-yl)benzoic acid | HCID 81111500 | — |
| Product | 2-(3,5-Dimethyl-1,2-oxazol-4-yl)-5-methylbenzoic acid | HCID 53225021 | — |
Reaction Steps
The title compound was synthesized following the same general protocol as described for 5-methyl-2-(1-methyl-1H-pyrazol-4-yl)benzoic acid in Example A1, using 3,5-dimethyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)isoxazole. ESI-MS (m/z): 232 [M+1]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09440982B2 |
| Source dataset | uspto-grants-2016_09 |
| ORD ID | ord-abe873709b86499fab59cf31e0553ee2 |
| Source note | uspto-grants-2016_09 |