HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methylpyridine-4-boronic acid pinacol ester → 5-Methyl-2-(2-methylpyridin-4-yl)benzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methylpyridine-4-boronic acid pinacol ester | HCID 16414274 | — |
| Reactant | 5-Methyl-2-(1-methyl-1H-pyrazol-4-yl)benzoic acid | HCID 81111500 | — |
| Product | 5-Methyl-2-(2-methylpyridin-4-yl)benzoic acid | HCID 116170039 | — |
Reaction Steps
The title compound was synthesized following the same general protocol as described for 5-methyl-2-(1-methyl-1H-pyrazol-4-yl)benzoic acid in Example A1, using 2-methyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridine. ESI-MS (m/z): 228 [M+1]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09440982B2 |
| Source dataset | uspto-grants-2016_09 |
| ORD ID | ord-1d2509a6735c4ab7b67cc05919320bca |
| Source note | uspto-grants-2016_09 |