HuagongsheHuagongshe Chemistry Print Report · For research reference only
(+-)-3-Quinuclidinol → HCID 15453400, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (+-)-3-Quinuclidinol | HCID 15381 | — |
| Reactant | 4-Methylphenyl isocyanate | HCID 69325 | — |
| Product | HCID 15453400 | HCID 15453400 | 93% |
Reaction Steps
3-Quinuclidinol and 4-tolyl isocyanate were used. Filtration of the precipitated solid from the cooled reaction mixture afforded the title compound (93%) as a white solid: mp 186.0-187.5° C.; FAB LRMS m /z (relative intensity, %) 262 (21), 261 ([MH+ ], 100).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05998429 |
| Source dataset | uspto-grants-1999_12 |
| ORD ID | ord-60f575926791426396557e5208a2edea |
| Source note | uspto-grants-1999_12 |