HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 21705551, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Water | HCID 962 | — |
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | 6-Bromohexanoic acid | HCID 20210 | — |
| Reactant | HCID 178527775 | HCID 178527775 | — |
| Product | HCID 21705551 | HCID 21705551 | — |
Reaction Steps
2-Mercaptobenzimidazole (6.3 g) and 6-bromocaproic acid (7.8 g) were dissolved in ethanol (35 ml), and the solution ws heated under reflux for 12 hours. After cooling, the reaction was added with water, and the mixture was adjusted to pH 8 with aqueous sodium carbonate. The deposited crystals were collected by filtration, and dried to obtain 11.2 g of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05998456 |
| Source dataset | uspto-grants-1999_12 |
| ORD ID | ord-7b171e35f35b4a2b8173ae3837c37287 |
| Source note | uspto-grants-1999_12 |