HRID610062

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID16477034

3-Amino-N-(4-fluorophenyl)benzamide

C13H11FN2O

结构：CCN1C(=O)C(C(=O)OC)c2cc(C3(C)OCCO3)ccc21

HCID53893352

未命名化合物

PRODUCTS

生成物

结构：CCN1C(=O)C(C(=O)Nc2cccc(C(=O)Nc3ccc(F)cc3)c2)c2cc(C(C)=O)ccc21

HCID9955841

未命名化合物

PROCEDURE

实验过程

Prepared as in Example 1 from 1-ethyl-5-(2-methyl-[1,3]dioxolan-2-yl)-2-oxo-2,3-dihydro-1H-indole-3-carboxylic acid methyl ester and 3-amino-N-(4-fluoro-phenyl)-benzamide. Recrystallized from ethyl acetate-hexanes-benzene. Calculated for C26H22FN3O4 : C 67.97; H 4.83; N 9.15; found C 68.34; H 5.31; N 8.80.

WORKUP

后处理

customRecrystallized from ethyl acetate-hexanes-benzene