HuagongsheHuagongshe Chemistry Print Report · For research reference only
Butyryl chloride → HCID 11044798, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Butyryl chloride | HCID 8855 | — |
| Reactant | 3-(1-Methyl-piperidin-4-yl)-1H-pyrrolo[3,2-b]pyridin-5-ylamine | HCID 10220230 | — |
| Product | HCID 11044798 | HCID 11044798 | 56.3% |
Reaction Steps
Beginning with 0.30 gm (1.3 mMol) 5-amino-3-(1-methylpiperidin-4-yl)pyrrolo[3,2-b]pyridine and 0.165 mL (1.56 mMol) butyryl chloride, 0.22 gm of the title compound were prepared as an ivory foam essentially by the procedure described in Example 4. This residue was crystallized from ethanol:water to provide material for analysis.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05998622 |
| Source dataset | uspto-grants-1999_12 |
| ORD ID | ord-4b8dce2ce7174e9b87bc02903dc577fd |
| Source note | uspto-grants-1999_12 |