HRID610737
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
1.2 g of fumaric acid was dissolved under heating in a mixture solvent of 100 cm3 of methanol and 12 cm3 of formic acid. After this solution was cooled to the normal temperature, into this solution, a further solution in which 3.38 g of formic acid copper was dissolved in 100 cm3 of methanol was dripped and then this was kept still for one day. Thereafter, the precipitation product was suction-filtered and dried for 120° C./4 hours, whereby 1.37 g of fumaric acid copper was obtained.
WORKUP
后处理
- temperatureAfter this solution was cooled to the normal temperature, into this solution
- filtrationThereafter, the precipitation product was suction-filtered
- customdried for 120° C./4 hours