Water → HCID 57285646, compound

Participants

Reaction Steps

Potassium monopersulfate (4.0 g), water (50 ml), and acetonitrile, (15 ml), were mixed together to form a solution. Then, ozone was added until the solution was saturated. A second solution of 1,3,5,7-tetra-aminocubane hydrochloride in water, 200 mg in 15 ml, was slowly added to the first solution while ozone was slowly bubbled through the first solution. The reaction temperature was 0 degrees C. The addition of ozone was stopped after 2 hours; the reaction mixture was stirred overnight and 10 ml of acetone were added.

Provenance & Evidence