Hydrochloric Acid → 1-(2-dimethylaminomethyl-6,7-dihydro-4H-furo[3,2-c]pyridin-5-yl)-3-(3-phenethylphenyl)propan-1-one hydrochloride

HRID 611104Notes

Reaction equation

HRID 611104 reaction equation
[CH3:1][N:2]([CH2:4][C:5]1[O:13][C:12]2[CH2:11][CH2:10][N:9]([C:14](=[O:31])[CH2:15][CH2:16][C:17]3[CH:22]=[CH:21][CH:20]=[C:19]([CH2:23][CH2:24][C:25]4[CH:30]=[CH:29][CH:28]=[CH:27][CH:26]=4)[CH:18]=3)[CH2:8][C:7]=2[CH:6]=1)[CH3:3].[ClH:32]>CO>[ClH:32].[CH3:1][N:2]([CH2:4][C:5]1[O:13][C:12]2[CH2:11][CH2:10][N:9]([C:14](=[O:31])[CH2:15][CH2:16][C:17]3[CH:22]=[CH:21][CH:20]=[C:19]([CH2:23][CH2:24][C:25]4[CH:30]=[CH:29][CH:28]=[CH:27][CH:26]=4)[CH:18]=3)[CH2:8][C:7]=2[CH:6]=1)[CH3:3]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 195999131-(2-dimethylaminomethyl-6,7-dihydro-4H-furo[3,2-c]pyridin-5-yl)-3-(3-phenethylphenyl)propan-1-one

Product 1

HCID 196002551-(2-dimethylaminomethyl-6,7-dihydro-4H-furo[3,2-c]pyridin-5-yl)-3-(3-phenethylphenyl)propan-1-one hydrochloride

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent2×

Procedure

1-(2-Dimethylaminomethyl-6,7-dihydro-4H-furo[3,2-c]pyridin-5-yl)-3-(3-phenethylphenyl)propan-1-one 0.293 g was dissolved in 2 ml of methanol; hydrogen chloride in methanol was added in excess, followed by stirring. This mixture was concentrated to yield the desired product.

Workup

  1. concentrationThis mixture was concentrated

Sources & evidence

ORD record
ord-a7b63dd0d9354e82ad151c4c424bbb76
Source dataset
uspto-grants-1999_12
Patent number
US05998433

Reaction notes

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