Hydrochloric Acid → HCID 19599900, compound

HRID 611179Notes

Reaction equation

HRID 611179 reaction equation
C(O[C:6]([N:8]([CH2:10][C:11]1[O:32][C:14]2[CH2:15][N:16]([C:19](=[O:31])[CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][C:25]3[CH:30]=[CH:29][CH:28]=[CH:27][CH:26]=3)[CH2:17][CH2:18][C:13]=2[CH:12]=1)C)=O)(C)(C)C.[ClH:33]>CO>[ClH:33].[CH3:6][NH:8][CH2:10][C:11]1[O:32][C:14]2[CH2:15][N:16]([C:19](=[O:31])[CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][C:25]3[CH:30]=[CH:29][CH:28]=[CH:27][CH:26]=3)[CH2:17][CH2:18][C:13]=2[CH:12]=1

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 19600129HCID 19600129, compound

Product 1

HCID 19599900HCID 19599900, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

1-[2-(N-tert-Butoxycarbonyl-N-methylaminomethyl)-5,7-dihydro-4H-furo[2,3-c]pyridin-6-yl]-6-phenylhexan-1-one 0.191 g was dissolved in 2 ml of methanol; 0.5 ml of concentrated hydrochloric acid was added, followed by stirring for 30 minutes. This mixture was concentrated to yield the desired product.

Workup

  1. concentrationThis mixture was concentrated

Sources & evidence

ORD record
ord-8cb15a09df9542f4ae2d5b819f351965
Source dataset
uspto-grants-1999_12
Patent number
US05998433

Reaction notes

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