Hydrochloric Acid → HCID 19600006, compound

HRID 611182Notes

Reaction equation

HRID 611182 reaction equation
[CH2:1]([N:3]([CH2:6][C:7]1[O:31][C:10]2[CH2:11][N:12]([C:15](=[O:30])[C:16]3[CH:21]=[CH:20][C:19]([C:22](=[O:29])[C:23]4[CH:28]=[CH:27][CH:26]=[CH:25][CH:24]=4)=[CH:18][CH:17]=3)[CH2:13][CH2:14][C:9]=2[CH:8]=1)[CH2:4][CH3:5])[CH3:2].[ClH:32]>CO>[ClH:32].[CH2:1]([N:3]([CH2:6][C:7]1[O:31][C:10]2[CH2:11][N:12]([C:15](=[O:30])[C:16]3[CH:21]=[CH:20][C:19]([C:22](=[O:29])[C:23]4[CH:28]=[CH:27][CH:26]=[CH:25][CH:24]=4)=[CH:18][CH:17]=3)[CH2:13][CH2:14][C:9]=2[CH:8]=1)[CH2:4][CH3:5])[CH3:2]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 19599902HCID 19599902, compound

Product 1

HCID 19600006HCID 19600006, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent2×

Procedure

N,N-Diethyl-[6-(4-benzoylbenzoyl)-4,5,6,7-tetrahydrofuro[2,3-c]pyridin-2-ylmethyl]amine 0.423 g was dissolved in 2 ml of methanol; hydrogen chloride in methanol was added in excess, followed by stirring. This mixture was concentrated to yield the desired product.

Workup

  1. concentrationThis mixture was concentrated

Sources & evidence

ORD record
ord-e6084c8bf0064144a3eeac7801f96614
Source dataset
uspto-grants-1999_12
Patent number
US05998433

Reaction notes

Loading…