Hydrochloric Acid → 1-(2-diethylaminomethyl-5,7-dihydro-4H-furo[2,3-c]pyridin-6-yl)-3-(3-phenethylphenyl)propan-1-one hydrochloride

HRID 611184Notes

Reaction equation

HRID 611184 reaction equation
[CH2:1]([N:3]([CH2:6][C:7]1[O:33][C:10]2[CH2:11][N:12]([C:15](=[O:32])[CH2:16][CH2:17][C:18]3[CH:23]=[CH:22][CH:21]=[C:20]([CH2:24][CH2:25][C:26]4[CH:31]=[CH:30][CH:29]=[CH:28][CH:27]=4)[CH:19]=3)[CH2:13][CH2:14][C:9]=2[CH:8]=1)[CH2:4][CH3:5])[CH3:2].[ClH:34]>CO>[ClH:34].[CH2:1]([N:3]([CH2:6][C:7]1[O:33][C:10]2[CH2:11][N:12]([C:15](=[O:32])[CH2:16][CH2:17][C:18]3[CH:23]=[CH:22][CH:21]=[C:20]([CH2:24][CH2:25][C:26]4[CH:27]=[CH:28][CH:29]=[CH:30][CH:31]=4)[CH:19]=3)[CH2:13][CH2:14][C:9]=2[CH:8]=1)[CH2:4][CH3:5])[CH3:2]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 196002351-(2-diethylaminomethyl-5,7-dihydro-4H-furo[2,3-c]pyridin-6-yl)-3-(3-phenethylphenyl)propan-1-one

Product 1

HCID 196002341-(2-diethylaminomethyl-5,7-dihydro-4H-furo[2,3-c]pyridin-6-yl)-3-(3-phenethylphenyl)propan-1-one hydrochloride

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent2×

Procedure

1-(2-Diethylaminomethyl-5,7-dihydro-4H-furo[2,3-c]pyridin-6-yl)-3-(3-phenethylphenyl)propan-1-one 0.208 g was dissolved in 2 ml of methanol; hydrogen chloride in methanol was added in excess, followed by stirring. This mixture was concentrated to yield the desired product.

Workup

  1. concentrationThis mixture was concentrated

Sources & evidence

ORD record
ord-8d3ec424a95943ffa9e540275bd062da
Source dataset
uspto-grants-1999_12
Patent number
US05998433

Reaction notes

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