Hydrochloric Acid → HCID 178483140, compound

HRID 611207Notes

Reaction equation

HRID 611207 reaction equation
[C:1]1([CH2:7][CH2:8][CH2:9][CH2:10][N-:11][C:12]([O:14][N:15]2[CH2:20][CH2:19][C:18]3[CH:21]=[C:22]([CH2:24][N:25]([CH3:27])[CH3:26])[O:23][C:17]=3[CH2:16]2)=[O:13])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[ClH:28]>CO>[ClH:28].[C:1]1([CH2:7][CH2:8][CH2:9][CH2:10][N-:11][C:12]([O:14][N:15]2[CH2:20][CH2:19][C:18]3[CH:21]=[C:22]([CH2:24][N:25]([CH3:27])[CH3:26])[O:23][C:17]=3[CH2:16]2)=[O:13])[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 178483139HCID 178483139, compound

Product 1

HCID 178483140HCID 178483140, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent2×

Procedure

N-(4-Phenylbutyl)-(2-dimethylaminomethyl-5,7-dihydro-4H-furo[2,3-c]pyridin-6-yl)carboxyamide 0.599 g was dissolved in 2 ml of methanol. To this solution, hydrogen chloride in methanol was added in excess, followed by stirring. This mixture was concentrated to yield the desired product.

Workup

  1. concentrationThis mixture was concentrated

Sources & evidence

ORD record
ord-92859623ff9044bebe8cea5d7c3aab30
Source dataset
uspto-grants-1999_12
Patent number
US05998433

Reaction notes

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