Hydrochloric Acid → HCID 19600143, compound

HRID 611214Notes

Reaction equation

HRID 611214 reaction equation
[CH2:1]([N:3]([CH2:6][C:7]1[O:15][C:14]2[CH2:13][CH2:12][N:11]([S:16]([CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][C:24]3[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=3)(=[O:18])=[O:17])[CH2:10][C:9]=2[CH:8]=1)[CH2:4][CH3:5])[CH3:2].[ClH:30]>CO>[ClH:30].[CH2:1]([N:3]([CH2:6][C:7]1[O:15][C:14]2[CH2:13][CH2:12][N:11]([S:16]([CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][C:24]3[CH:25]=[CH:26][CH:27]=[CH:28][CH:29]=3)(=[O:18])=[O:17])[CH2:10][C:9]=2[CH:8]=1)[CH2:4][CH3:5])[CH3:2]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 19600144HCID 19600144, compound

Product 1

HCID 19600143HCID 19600143, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent2×

Procedure

N,N-Diethyl-[5-(5-phenylpentylsulfonyl)-4,5,6,7-tetrahydrofuro[3,2-c]pyridin-2-ylmethyl]amine 0.168 g was dissolved in 2 ml of methanol; hydrogen chloride in methanol was added in excess, followed by stirring. This mixture was concentrated to yield the desired product.

Workup

  1. concentrationThis mixture was concentrated

Sources & evidence

ORD record
ord-76fabec0e4a7463f827bea01aa6ab11d
Source dataset
uspto-grants-1999_12
Patent number
US05998433

Reaction notes

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