Hydrochloric Acid → HCID 19600080, compound

HRID 611219Notes

Reaction equation

HRID 611219 reaction equation
[CH3:1][N:2]([CH2:4][C:5]1[O:26][C:8]2[CH2:9][N:10]([CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][C:20]3[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=3)[CH2:11][CH2:12][CH2:13][C:7]=2[CH:6]=1)[CH3:3].[ClH:27]>CO>[ClH:27].[ClH:27].[CH3:1][N:2]([CH2:4][C:5]1[O:26][C:8]2[CH2:9][N:10]([CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][C:20]3[CH:21]=[CH:22][CH:23]=[CH:24][CH:25]=3)[CH2:11][CH2:12][CH2:13][C:7]=2[CH:6]=1)[CH3:3]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 19599959HCID 19599959, compound

Product 1

HCID 19600080HCID 19600080, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent2×

Procedure

N,N-Dimethyl-[7-(6-phenylhexyl)-5,6,7,8-tetrahydro-4H-furo[2,3-c]azepin-2-ylmethyl]amine 0.739 g was dissolved in 2 ml of methanol; hydrogen chloride in methanol was added in excess, followed by stirring. This mixture was concentrated to yield the desired product.

Workup

  1. concentrationThis mixture was concentrated

Sources & evidence

ORD record
ord-2a699fa9cb28490f865ea427650e4ca4
Source dataset
uspto-grants-1999_12
Patent number
US05998433

Reaction notes

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