Hydrochloric Acid → HCID 19600075, compound

HRID 611224Notes

Reaction equation

HRID 611224 reaction equation
[CH3:1][N:2]([CH2:4][C:5]1[O:30][C:8]2[CH2:9][N:10]([C:14](=[O:29])[C:15]3[CH:20]=[CH:19][C:18]([C:21](=[O:28])[C:22]4[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=4)=[CH:17][CH:16]=3)[CH2:11][CH2:12][CH2:13][C:7]=2[CH:6]=1)[CH3:3].[ClH:31]>CO>[ClH:31].[CH3:3][N:2]([CH2:4][C:5]1[O:30][C:8]2[CH2:9][N:10]([C:14](=[O:29])[C:15]3[CH:20]=[CH:19][C:18]([C:21](=[O:28])[C:22]4[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=4)=[CH:17][CH:16]=3)[CH2:11][CH2:12][CH2:13][C:7]=2[CH:6]=1)[CH3:1]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 19600045HCID 19600045, compound

Product 1

HCID 19600075HCID 19600075, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent2×

Procedure

N,N-Dimethyl-[7-(4-benzoylbenzoyl)-5,6,7,8-tetrahydro-4H-furo[2,3-c]azepin-2-ylmethyl]amine 0.166 g was dissolved in 2 ml of methanol; hydrogen chloride in methanol was added in excess, followed by stirring. This mixture was concentrated to yield the desired product.

Workup

  1. concentrationThis mixture was concentrated

Sources & evidence

ORD record
ord-da4e943cb4bc475ca84e7b59353d0528
Source dataset
uspto-grants-1999_12
Patent number
US05998433

Reaction notes

Loading…