HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 19600204, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 19600009 | HCID 19600009 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 19600204 | HCID 19600204 | — |
Reaction Steps
To a solution of 0.148 g of 1-[2-(2-oxazolin-2-yl)-5,7-dihydro-4H-furo[2,3-c]pyridin-6-yl]-6-phenylhexan-1-one in 10 ml of diethyl ether, 0.5 ml of about 10% hydrogen chloride in methanol was added, followed by stirring for 10 minutes, after which the solvent was distilled off under reduced pressure. The resulting crude product was crystallized from diethyl ether to yield the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05998433 |
| Source dataset | uspto-grants-1999_12 |
| ORD ID | ord-332d630ae3d04deb8a4e1a025f9d35e2 |
| Source note | uspto-grants-1999_12 |