Hydrochloric Acid → HCID 19600223, compound

HRID 611250Notes

Reaction equation

HRID 611250 reaction equation
[CH3:1][O:2][CH2:3][CH2:4][N:5]([CH2:7][C:8]1[O:32][C:11]2[CH2:12][N:13]([C:16](=[O:31])[C:17]3[CH:22]=[CH:21][C:20]([C:23](=[O:30])[C:24]4[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=4)=[CH:19][CH:18]=3)[CH2:14][CH2:15][C:10]=2[CH:9]=1)[CH3:6].[ClH:33]>CO>[ClH:33].[CH3:1][O:2][CH2:3][CH2:4][N:5]([CH2:7][C:8]1[O:32][C:11]2[CH2:12][N:13]([C:16](=[O:31])[C:17]3[CH:22]=[CH:21][C:20]([C:23](=[O:30])[C:24]4[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=4)=[CH:19][CH:18]=3)[CH2:14][CH2:15][C:10]=2[CH:9]=1)[CH3:6]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 19600105HCID 19600105, compound

Product 1

HCID 19600223HCID 19600223, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent2×

Procedure

N-(2-Methoxyethyl)-N-methyl-[6-(4-benzoylbenzoyl)-4,5,6,7-tetrahydrofuro[2,3-c]pyridin-2-ylmethyl]amine 0.322 g was dissolved in 2 ml of methanol; hydrogen chloride in methanol was added in excess, followed by stirring. The resulting mixture was then concentrated to yield the desired product.

Workup

  1. concentrationThe resulting mixture was then concentrated

Sources & evidence

ORD record
ord-0c0391c5395c4c2590eb9c3e98c6399d
Source dataset
uspto-grants-1999_12
Patent number
US05998433

Reaction notes

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