Hydrochloric Acid → HCID 19599932, compound

HRID 611252Notes

Reaction equation

HRID 611252 reaction equation
[C:1]([C:9]1[CH:31]=[CH:30][C:12]([C:13]([N:15]2[CH2:20][CH2:19][C:18]3[CH:21]=[C:22]([CH2:24][N:25]4[CH2:29][CH2:28][CH2:27][CH2:26]4)[O:23][C:17]=3[CH2:16]2)=[O:14])=[CH:11][CH:10]=1)(=[O:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[ClH:32]>CO>[ClH:32].[C:1]([C:9]1[CH:31]=[CH:30][C:12]([C:13]([N:15]2[CH2:20][CH2:19][C:18]3[CH:21]=[C:22]([CH2:24][N:25]4[CH2:26][CH2:27][CH2:28][CH2:29]4)[O:23][C:17]=3[CH2:16]2)=[O:14])=[CH:11][CH:10]=1)(=[O:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 19599933HCID 19599933, compound

Product 1

HCID 19599932HCID 19599932, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent2×

Procedure

6-(4-Benzoylbenzoyl)-2-(1-pyrrolidinylmethyl)-4,5,6,7-tetrahydrofuro[2,3-c]pyridine 0.225 g was dissolved in 2 ml of methanol; hydrogen chloride in methanol was added in excess, followed by stirring. The resulting mixture was then concentrated to yield the desired product.

Workup

  1. concentrationThe resulting mixture was then concentrated

Sources & evidence

ORD record
ord-ba7201cd469e4cd3bd3ad17fc1c32566
Source dataset
uspto-grants-1999_12
Patent number
US05998433

Reaction notes

Loading…