Hydrochloric Acid → HCID 19600228, compound

HRID 611254Notes

Reaction equation

HRID 611254 reaction equation
[C:1]([C:9]1[CH:32]=[CH:31][C:12]([C:13]([N:15]2[CH2:20][CH2:19][C:18]3[CH:21]=[C:22]([CH2:24][N:25]4[CH2:30][CH2:29][CH2:28][CH2:27][CH2:26]4)[O:23][C:17]=3[CH2:16]2)=[O:14])=[CH:11][CH:10]=1)(=[O:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[ClH:33]>CO>[ClH:33].[C:1]([C:9]1[CH:32]=[CH:31][C:12]([C:13]([N:15]2[CH2:20][CH2:19][C:18]3[CH:21]=[C:22]([CH2:24][N:25]4[CH2:26][CH2:27][CH2:28][CH2:29][CH2:30]4)[O:23][C:17]=3[CH2:16]2)=[O:14])=[CH:11][CH:10]=1)(=[O:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 19599984HCID 19599984, compound

Product 1

HCID 19600228HCID 19600228, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent2×

Procedure

6-(4-Benzoylbenzoyl)-2-piperidinomethyl-4,5,6,7-tetrahydrofuro[2,3-c]pyridine 0.297 g was dissolved in 2 ml of methanol; hydrogen chloride in methanol was added in excess, followed by stirring. This was concentrated to yield the desired product.

Workup

  1. concentrationThis was concentrated

Sources & evidence

ORD record
ord-d43c951eaca045a39079fcd4e91053c6
Source dataset
uspto-grants-1999_12
Patent number
US05998433

Reaction notes

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