Hydrochloric Acid → HCID 19599930, compound

HRID 611278Notes

Reaction equation

HRID 611278 reaction equation
[CH2:1]([N:3]([CH2:6][C:7]1[O:32][C:10]2[CH2:11][N:12]([C:15](=[O:31])[C:16]3[CH:21]=[CH:20][C:19]([C:22](=[O:30])[C:23]4[CH:28]=[CH:27][C:26]([Cl:29])=[CH:25][CH:24]=4)=[CH:18][CH:17]=3)[CH2:13][CH2:14][C:9]=2[CH:8]=1)[CH2:4][CH3:5])[CH3:2].Cl>CO>[ClH:29].[CH2:1]([N:3]([CH2:6][C:7]1[O:32][C:10]2[CH2:11][N:12]([C:15](=[O:31])[C:16]3[CH:21]=[CH:20][C:19]([C:22](=[O:30])[C:23]4[CH:24]=[CH:25][C:26]([Cl:29])=[CH:27][CH:28]=4)=[CH:18][CH:17]=3)[CH2:13][CH2:14][C:9]=2[CH:8]=1)[CH2:4][CH3:5])[CH3:2]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 19599931HCID 19599931, compound

Product 1

HCID 19599930HCID 19599930, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent2×

Procedure

N,N-Diethyl-[6-[4-(4-chlorobenzoyl)benzoyl]-4,5,6,7-tetrahydrofuro[2,3-c]pyridin-2-ylmethyl]amine 1.047 g was dissolved in 2 ml of methanol; hydrogen chloride in methanol was added in excess, followed by stirring. This was concentrated to yield the desired product.

Workup

  1. concentrationThis was concentrated

Sources & evidence

ORD record
ord-f2e8e56667ca4d0c95351e258387fb9c
Source dataset
uspto-grants-1999_12
Patent number
US05998433

Reaction notes

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