Hydrochloric Acid → HCID 19600094, compound

HRID 611307Notes

Reaction equation

HRID 611307 reaction equation
[CH3:1][N:2]([CH2:4][C:5]1[O:28][C:8]2[CH2:9][N:10]([C:13](=[O:27])[C:14]3[CH:19]=[CH:18][C:17]([C:20]([C:22]4[O:23][CH:24]=[CH:25][CH:26]=4)=[O:21])=[CH:16][CH:15]=3)[CH2:11][CH2:12][C:7]=2[CH:6]=1)[CH3:3].[ClH:29]>CO>[ClH:29].[CH3:3][N:2]([CH2:4][C:5]1[O:28][C:8]2[CH2:9][N:10]([C:13](=[O:27])[C:14]3[CH:15]=[CH:16][C:17]([C:20]([C:22]4[O:23][CH:24]=[CH:25][CH:26]=4)=[O:21])=[CH:18][CH:19]=3)[CH2:11][CH2:12][C:7]=2[CH:6]=1)[CH3:1]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 19599888HCID 19599888, compound

Product 1

HCID 19600094HCID 19600094, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent2×

Procedure

N,N-Dimethyl-[6-[4-(2-furoyl)benzoyl]-4,5,6,7-tetrahydrofuro[2,3-c]pyridin-2-ylmethyl]amine 0.310 g was dissolved in 2 ml of methanol; hydrogen chloride in methanol was added in excess, followed by stirring. This mixture was then concentrated to yield the desired product.

Workup

  1. concentrationThis mixture was then concentrated

Sources & evidence

ORD record
ord-048106f4e2b94cab93e413606fe337fc
Source dataset
uspto-grants-1999_12
Patent number
US05998433

Reaction notes

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