HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 6-[4-(1-Phenylethenyl)benzoyl]-2-(1-pyrrolidinylmethyl)-4,5,6,7-tetrahydrofuro[2,3-c]pyridine hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 6-[4-(1-Phenylethenyl)benzoyl]-2-(1-pyrrolidinylmethyl)-4,5,6,7-tetrahydrofuro[2,3-c]pyridine | HCID 19599962 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 6-[4-(1-Phenylethenyl)benzoyl]-2-(1-pyrrolidinylmethyl)-4,5,6,7-tetrahydrofuro[2,3-c]pyridine hydrochloride | HCID 19600116 | — |
Reaction Steps
6-[4-(1-Phenylethenyl)benzoyl]-2-(1-pyrrolidinylmethyl)-4,5,6,7-tetrahydrofuro[2,3-c]pyridine 0.688 g was dissolved in 2 ml of methanol and hydrogen chloride in methanol was added in excess, followed by stirring. This mixture was concentrated to yield the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05998433 |
| Source dataset | uspto-grants-1999_12 |
| ORD ID | ord-2b203cbe85fe4e38a523d5387ae45cfe |
| Source note | uspto-grants-1999_12 |