Hydrochloric Acid → HCID 67585952, compound

HRID 611412Notes

Reaction equation

HRID 611412 reaction equation
[CH3:1][N:2]([CH2:4][C:5]1[O:13][C:12]2[CH2:11][CH2:10][N:9]([S:14]([C:17]3[CH:22]=[CH:21][C:20](/[CH:23]=[CH:24]\[C:25]4[CH:30]=[CH:29][CH:28]=[CH:27][CH:26]=4)=[CH:19][CH:18]=3)(=[O:16])=[O:15])[CH2:8][C:7]=2[CH:6]=1)[CH3:3].[ClH:31]>CO>[ClH:31].[CH3:1][N:2]([CH2:4][C:5]1[O:13][C:12]2[CH2:11][CH2:10][N:9]([S:14]([C:17]3[CH:22]=[CH:21][C:20](/[CH:23]=[CH:24]\[C:25]4[CH:30]=[CH:29][CH:28]=[CH:27][CH:26]=4)=[CH:19][CH:18]=3)(=[O:16])=[O:15])[CH2:8][C:7]=2[CH:6]=1)[CH3:3]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 67585953HCID 67585953, compound

Product 1

HCID 67585952HCID 67585952, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent2×

Procedure

(Z)-N,N-Dimethyl-[5-(4-stilbenesulfonyl)-4,5,6,7-tetrahydrofuro[3,2-c]pyridin-2-ylmethyl]amine 0.148 g was dissolved in 2 ml of methanol; hydrogen chloride in methanol was added in excess, followed by stirring. This mixture was concentrated to yield the desired product.

Workup

  1. concentrationThis mixture was concentrated

Sources & evidence

ORD record
ord-2a9eed23bf77413daa20f9cea0b4814d
Source dataset
uspto-grants-1999_12
Patent number
US05998433

Reaction notes

Loading…