Hydrochloric Acid → HCID 67585069, compound

HRID 611420Notes

Reaction equation

HRID 611420 reaction equation
[CH3:1][N:2]([CH2:4][C:5]1[O:13][C:12]2[CH2:11][CH2:10][N:9]([S:14]([C:17]3[CH:31]=[CH:30][C:20](/[CH:21]=[CH:22]\[C:23]4[CH:28]=[CH:27][CH:26]=[C:25]([Cl:29])[CH:24]=4)=[CH:19][CH:18]=3)(=[O:16])=[O:15])[CH2:8][C:7]=2[CH:6]=1)[CH3:3].Cl>CO>[ClH:29].[CH3:1][N:2]([CH2:4][C:5]1[O:13][C:12]2[CH2:11][CH2:10][N:9]([S:14]([C:17]3[CH:31]=[CH:30][C:20](/[CH:21]=[CH:22]\[C:23]4[CH:28]=[CH:27][CH:26]=[C:25]([Cl:29])[CH:24]=4)=[CH:19][CH:18]=3)(=[O:16])=[O:15])[CH2:8][C:7]=2[CH:6]=1)[CH3:3]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 67584930HCID 67584930, compound

Product 1

HCID 67585069HCID 67585069, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent2×

Procedure

(Z)-N,N-Dimethyl-[5-(3-chlorostilbene-4'-sulfonyl)-4,5,6,7-tetrahydrofuro[3,2-c]pyridin-2-ylmethyl]amine 0.390 g was dissolved in 2 ml of methanol; hydrogen chloride in methanol was added in excess, followed by stirring. This mixture was concentrated; the resulting solid was washed with diethyl ether to yield the desired product.

Workup

  1. concentrationThis mixture was concentrated
  2. washthe resulting solid was washed with diethyl ether

Sources & evidence

ORD record
ord-0e7aa9f0963b4b4797e763192fdb670a
Source dataset
uspto-grants-1999_12
Patent number
US05998433

Reaction notes

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