Hydrochloric Acid → HCID 67585203, compound

HRID 611424Notes

Reaction equation

HRID 611424 reaction equation
[CH3:1][N:2]([CH2:4][C:5]1[O:13][C:12]2[CH2:11][CH2:10][N:9]([S:14]([C:17]3[CH:31]=[CH:30][C:20](/[CH:21]=[CH:22]\[C:23]4[CH:28]=[CH:27][C:26]([Cl:29])=[CH:25][CH:24]=4)=[CH:19][CH:18]=3)(=[O:16])=[O:15])[CH2:8][C:7]=2[CH:6]=1)[CH3:3].Cl>CO>[ClH:29].[CH3:1][N:2]([CH2:4][C:5]1[O:13][C:12]2[CH2:11][CH2:10][N:9]([S:14]([C:17]3[CH:31]=[CH:30][C:20](/[CH:21]=[CH:22]\[C:23]4[CH:24]=[CH:25][C:26]([Cl:29])=[CH:27][CH:28]=4)=[CH:19][CH:18]=3)(=[O:15])=[O:16])[CH2:8][C:7]=2[CH:6]=1)[CH3:3]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 67585204HCID 67585204, compound

Product 1

HCID 67585203HCID 67585203, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent2×

Procedure

(Z)-N,N-Dimethyl-[5-(4-chlorostilbene-4'-sulfonyl)-4,5,6,7-tetrahydrofuro[3,2-c]pyridin-2-ylmethyl]amine 0.652 g was dissolved in 2 ml of methanol; hydrogen chloride in methanol was added in excess, followed by stirring. This mixture was concentrated to yield the desired product.

Workup

  1. concentrationThis mixture was concentrated

Sources & evidence

ORD record
ord-487d27670e034d3ea48d0d8ed354e8a6
Source dataset
uspto-grants-1999_12
Patent number
US05998433

Reaction notes

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