HRID611431

反应详情

EQUATION

反应方程式

HRID 611431 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

2-Dimethylaminomethyl-5-(6-phenylhexyl)-6,7-dihydro-5H-furo[3,2-c]pyridin-4-one 0.159 g was dissolved in 2 ml of methanol; hydrogen chloride in methanol was added in excess, followed by stirring. This mixture was concentrated; the resulting solid was washed with diethyl ether to yield the desired product.

WORKUP

后处理

  1. concentrationThis mixture was concentrated
  2. washthe resulting solid was washed with diethyl ether