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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 611489Generated: October 31, 2026

Acetic Acid → HCID 178467663, compound

https://huagongshe.com/reaction/611489

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAcetic AcidHCID 176—
ReactantTriphenylphosphineHCID 11776—
ReactantHCID 19597260HCID 19597260—
ProductHCID 178467663HCID 178467663—

Reaction Steps

A solution of 3-[2-[(diethoxyphosphoryl)acetyl]hydrazino]-1-hydroxy-6-(4-methyl-2-phenyl-1H-imidazol-1-yl)-7-trifluoromethylquinoxalin-2(1H)-one (1.5 g, 2.5 mmol) and triphenylphosphine (1.3 g, 5 mmol) in 50 ml of glacial acetic acid was stirred overnight at 120° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06001832
Source datasetuspto-grants-1999_12
ORD IDord-7d1fbb6825cd4e77979673b93bd48e84
Source noteuspto-grants-1999_12