HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 70204452, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Methanol | HCID 887 | — |
| Reactant | Water | HCID 962 | — |
| Reactant | tert-butyl (2R)-2-ethynylpyrrolidine-1-carboxylate | HCID 10262067 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 70204452 | HCID 70204452 | — |
Reaction Steps
The title compound was prepared from 1-Boc-2(R)-ethynylpyrrolidine according to the procedures of Example 5 above: [α]D≤ +16.5° (c 1.0, MeOH); Anal. Calcd for C12H14N2O.2.0 HCl.0.2 H2O.0.2 ethanol: C, 51.39; H, 6.19; N, 9.67. Found: C, 51.63; H, 6.49; N, 9.33.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06001849 |
| Source dataset | uspto-grants-1999_12 |
| ORD ID | ord-cf18250a4d0442579d0a156b79271f9c |
| Source note | uspto-grants-1999_12 |