HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thiophenol → HCID 18470180, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thiophenol | HCID 7969 | — |
| Reactant | 1,7-Dibromoheptane | HCID 78309 | — |
| Reactant | 7-Phenoxyheptyl bromide | HCID 10516252 | — |
| Product | HCID 18470180 | HCID 18470180 | 46% |
Reaction Steps
7-Phenylthioheptyl bromide was prepared from thiophenol (4.40 g, 40 mmol) and 1,7-dibromoheptane (10.32 g, 40 mmol) as described above for 7-phenoxyheptyl bromide. Yield: 46% bp; 132-136° C./0.05 torr; 1H-NMR: 1.30-1.85 (m, 10 H), 2.90 (t, 2 H), 3.35 (t, 2 H), 7.25 (s, 5 H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06001869 |
| Source dataset | uspto-grants-1999_12 |
| ORD ID | ord-19b34db99280459bb0b5eded759013c2 |
| Source note | uspto-grants-1999_12 |