HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 19598113, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 19598101 | HCID 19598101 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 19598113 | HCID 19598113 | — |
Reaction Steps
A mixture of 66A (6.65 g), potassium carbonate (7.0 g), water (50 ml) and methanol (100 ml) is heated to reflux for 3 hours. Upon cooling to room temperature water is added. The reaction mixture is filtered and the filtrate is acidified with concentrated hydrochloric acid. The solid material is collected and used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06001883 |
| Source dataset | uspto-grants-1999_12 |
| ORD ID | ord-bbe46ee6f7564ed5b3b090e5fd62b9c0 |
| Source note | uspto-grants-1999_12 |