HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenyl isocyanate → HCID 19598330, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenyl isocyanate | HCID 7672 | — |
| Reactant | 1-(Aminooxy)-3-(piperidin-1-yl)propan-2-ol | HCID 18766210 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 19598330 | HCID 19598330 | — |
Reaction Steps
O-(2-hydroxy-3-piperidino-propyl)-hydroxylamine (1,74 g, 0,01 mol) was dissolved in 40 ml chloroform and 1,09 ml (0,01 mol) phenyl isocyanate was added thereto while stirring. The reaction was monitored by chromatography. After the end of reaction the solution was evaporated and the oily residue was purified by column chromatography. The oil thus obtained was crystallized from diethyl ether. Yield: 0,6 g (20%). Mp: 101-103° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06002002 |
| Source dataset | uspto-grants-1999_12 |
| ORD ID | ord-bcaa123d1a6f41e8a491081e22ef3387 |
| Source note | uspto-grants-1999_12 |