HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropyl isocyanate → HCID 19598328, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropyl isocyanate | HCID 61277 | — |
| Reactant | 1-(Aminooxy)-3-(piperidin-1-yl)propan-2-ol | HCID 18766210 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 19598328 | HCID 19598328 | — |
Reaction Steps
O-(2-hydroxy-3-piperidino-propyl)-hydroxylamine (1,74 g, 0,01 mol) was dissolved in 25 ml abs. chloroform and under stirring, 0,98 ml (0,01 mol) isopropyl isocyanate was added. The reaction was monitored by chromatography. At the end of the reaction the solution was evaporated and the oily residue purified by column chromatography. The oil thus obtained was crystallized with methanol-ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06002002 |
| Source dataset | uspto-grants-1999_12 |
| ORD ID | ord-ee156c9509bc47a595b6e51d72ce0b77 |
| Source note | uspto-grants-1999_12 |