HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl isocyanate → HCID 19598322, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl isocyanate | HCID 76639 | — |
| Reactant | 1-(Aminooxy)-3-(piperidin-1-yl)propan-2-ol | HCID 18766210 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 19598322 | HCID 19598322 | — |
Reaction Steps
O-(2-hydroxy-3-piperidino-propyl)-hydroxylamine (2,53 g, 0,0145 mol) was dissolved in 40 ml abs. chloroform and 1,8 ml (0,0145 mol) benzyl isocyanate was added thereto while stirring. The mixture was stirred for 2 hours, the solution was evaporated and the residue was crystallized from ethanol-ether mixture. Yield: 2,1 g (47%). Mp.: 100-101° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06002002 |
| Source dataset | uspto-grants-1999_12 |
| ORD ID | ord-95b48cfbc99a45f98ab4dc31fd79ed96 |
| Source note | uspto-grants-1999_12 |