HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Nitrophenyl isocyanate → HCID 9797937, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Nitrophenyl isocyanate | HCID 76835 | — |
| Reactant | 1-(Aminooxy)-3-(piperidin-1-yl)propan-2-ol | HCID 18766210 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 9797937 | HCID 9797937 | — |
Reaction Steps
O-(2-hydroxy-3-piperidino-propyl)-hydroxylamine (1,74 g, 0,01 mol) was dissolved in 25 ml abs. chloroform and 1,64 g (0,01 mol) 3-nitrophenyl isocyanate in 20 ml abs. chloroform was added thereto while stirring. After 1 hour reaction the mixture was evaporated and purified by column chromatography. The oil thus obtained was crystallized from diethyl ether. Yield: 1,84 g (54%). Mp.: 137-139° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06002002 |
| Source dataset | uspto-grants-1999_12 |
| ORD ID | ord-d5d8c754dbd8454582f0546f74fc4cfe |
| Source note | uspto-grants-1999_12 |