HCID 178418361, compound → HCID 178500031, compound

HRID 611790Notes

Reaction equation

HRID 611790 reaction equation
[NH:1]1[CH:5]=[C:4]([CH:6]=[CH:7][C:8]([O:10][CH3:11])=[O:9])[N:3]=[CH:2]1.[H][H]>CO.[Pd]>[NH:1]1[CH:5]=[C:4]([CH2:6][CH2:7][C:8]([O:10][CH3:11])=[O:9])[N:3]=[CH:2]1

Participants

5

Reactant 2

HCID 178418361HCID 178418361, compoundHCID 178500030HCID 178500030, compound

Product 1

HCID 178500031HCID 178500031, compound

Reagents, catalysts & solvents 2

HCID 23938PalladiumCatalystHCID 887MethanolSolvent

Procedure

To a solution of methyl 3-(4-imidazolyl)-2-propenoate (5.3 g) in methanol a t room temperature was added 10% palladium on carbon (20 mg) under a blanket of argon. A balloon of hydrogen was applied, and the reaction was stirred for one hour. The solution was filtered, and then concentrated in vacuo to dryness to provide the title compound.

Workup

  1. filtrationThe solution was filtered
  2. concentrationconcentrated in vacuo to dryness

Sources & evidence

ORD record
ord-3d606444b5ca4c0b8d6a7889e527d926
Source dataset
uspto-grants-1999_12
Patent number
US06001835

Reaction notes

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