HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178418361, compound → HCID 178500031, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Reactant | HCID 178500030 | HCID 178500030 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178500031 | HCID 178500031 | — |
Reaction Steps
To a solution of methyl 3-(4-imidazolyl)-2-propenoate (5.3 g) in methanol a t room temperature was added 10% palladium on carbon (20 mg) under a blanket of argon. A balloon of hydrogen was applied, and the reaction was stirred for one hour. The solution was filtered, and then concentrated in vacuo to dryness to provide the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06001835 |
| Source dataset | uspto-grants-1999_12 |
| ORD ID | ord-3d606444b5ca4c0b8d6a7889e527d926 |
| Source note | uspto-grants-1999_12 |