Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Toluene | HCID 1140 | — |
| Reactant | Methyl fluorosulfate | HCID 9870 | — |
| Reactant | HCID 14459514 | HCID 14459514 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 14459515 | HCID 14459515 | — |
Reaction Steps
0.4 ml of methyl fluorosulfonate is added at -20° C. to 1.27 g of (5) in 60 ml of dichloromethane. The mixture is left to stir at -20° C. for 2 hours and to reach room ##STR17## temperature overnight. Addition of toluene results in precipitation of a yellow solid which is filtered off with suction and dried in vacuo.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06002007 |
|---|
| Source dataset | uspto-grants-1999_12 |
|---|
| ORD ID | ord-fc400cb87bae4240bd8449e127d99e1a |
|---|
| Source note | uspto-grants-1999_12 |
|---|
