Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 612318Generated: October 31, 2026

3,4-Dimethylaniline → HCID 19593892, compound

https://huagongshe.com/reaction/612318

Reaction equation

Participants

RoleNameHCIDCharge
Reactant3,4-DimethylanilineHCID 7248—
Reactant2-MethylcyclohexanoneHCID 11419—
ReactantHCID 178418385HCID 178418385—
ProductHCID 19593892HCID 19593892—

Reaction Conditions

Temperature120 °C

Reaction Steps

In a 100-mL flask, the following mixture is heated at 120° C. for 24 h: 12 g 3,4-dimethylaniline, 11 g 2-methylcyclohexanone and 12 g benzotriazole. The 2-methylcyclohexyl-2,4-dimethylphenylamine is isolated after reduction, as in step 1 of Example 1. 18 g of an oily product are isolated.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06004486
Source datasetuspto-grants-1999_12
ORD IDord-332d337a133e4ded86b045c7aee1e363
Source noteuspto-grants-1999_12