HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromo-1,1,1-trifluoroethane → HCID 178447746, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromo-1,1,1-trifluoroethane | HCID 67898 | — |
| Reactant | (4-Pentyl-4-phenyl-4-silacyclohexyl)methyltriphenylphosphonium iodide | HCID 19593804 | — |
| Reactant | 4'-Formyl-3-fluoro-4-(t-butyldimethylsiloxy)biphenyl | HCID 19593836 | — |
| Product | HCID 178447746 | HCID 178447746 | — |
Reaction Steps
The general procedure of Example 56 was repeated using (4-pentyl-4-phenyl-4-silacyclohexyl)methyltriphenylphosphonium iodide, 4'-formyl-3-fluoro-4-(t-butyldimethylsiloxy)biphenyl and 1-bromo-2, 2,2-trifluoroethane, thereby obtaining the intended compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06004478 |
| Source dataset | uspto-grants-1999_12 |
| ORD ID | ord-d676946764974369a06beb395fdad7b3 |
| Source note | uspto-grants-1999_12 |