HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-butyl N-(2-hydroxyethyl)carbamate → HCID 19596585, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-butyl N-(2-hydroxyethyl)carbamate | HCID 2733206 | — |
| Reactant | HCID 178519005 | HCID 178519005 | — |
| Product | HCID 19596585 | HCID 19596585 | 74.1% |
Reaction Steps
4-Chloro-3-hydroxy-5-(2-thienyl)isoxazole (0.50 g) and 2-(N-tert-butoxycarbonylamino)ethanol (0.40 g) were subjected to reaction and post-treatment in a similar manner to that described in Example 1(a) to obtain the title compound (0.57 g, 66%) as colorless crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06005116 |
| Source dataset | uspto-grants-1999_12 |
| ORD ID | ord-e452918cb91f49529da523ee82f28b43 |
| Source note | uspto-grants-1999_12 |