HCID 19596650, compound → HCID 19596632, compound

Participants

Reaction Steps

3-(2-(N-tert-Butoxycarbonylamino)ethoxy)-5-(2-methoxyphenyl)isoxazole (0.31 g) was dissolved in a solution of 4N hydrochloric acid/1,4-dioxane (2.3 ml), and the solution was stirred at room temperature for 30 minutes. The solvent was evaporated under reduced pressure and the residue was recrystallized from a mixture of ethanol and isopropanol to obtain the title compound (0.21 g, 84%) as colorless crystals.

Provenance & Evidence