HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydroxyamine hydrochloride → HCID 178518997, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydroxyamine hydrochloride | HCID 443297 | — |
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | HCID 11557587 | HCID 11557587 | — |
| Product | HCID 178518997 | HCID 178518997 | 39% |
Reaction Steps
2-Benzoyl-2-cyclopropylacetic acid methyl ester (0.9 g), hydroxylamine hydrochloride (0.6 g) and sodium methoxide (28% methanol solution, 4.0 ml) were subjected to reaction and post-treatment in a similar manner to that described in Reference example 8(b) to obtain the title compound (0.32 g, 39%) as colorless crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06005116 |
| Source dataset | uspto-grants-1999_12 |
| ORD ID | ord-522ba5938b954c5d8de4ffc80ac8332e |
| Source note | uspto-grants-1999_12 |