Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 612966Generated: October 30, 2026

Hydroxyamine hydrochloride → HCID 178439788, compound

https://huagongshe.com/reaction/612966

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydroxyamine hydrochlorideHCID 443297—
ReactantSodium MethoxideHCID 10942334—
ReactantHCID 53640330HCID 53640330—
ProductHCID 178439788HCID 17843978823%

Reaction Steps

2-Nicotinoylisovaleric acid ethyl ester (0.76 g), hydroxylamine hydrochloride (0.46 g) and sodium methoxide (28% methanol solution, 3.1 ml) were subjected to reaction and post-treatment in a similar manner to that described in Reference example 8(b) to obtain the title compound (0.15 g, 23%) as colorless crystals.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06005116
Source datasetuspto-grants-1999_12
ORD IDord-64da0e24ee5e4e77b755434508f36e44
Source noteuspto-grants-1999_12