Hydrochloric Acid → HCID 13063265, compound

HRID 613362Notes

Reaction equation

HRID 613362 reaction equation
[C:1]1([NH:7][CH2:8][C:9]([OH:11])=[O:10])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[ClH:12].[CH3:13][CH2:14]O>>[ClH:12].[CH2:13]([N:7]([C:1]1[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1)[CH2:8][C:9]([OH:11])=[O:10])[CH3:14]

Participants

4

Reactant 3

HCID 313Hydrochloric AcidHCID 702EthanolHCID 66025N-Phenylglycine

Product 1

HCID 13063265HCID 13063265, compound

Procedure

To a mixture of phenylglycine (15.00 gram (hereinafter g.), 0.1 mole (hereinafter mol)) in EtOH (100 miliLiters (hereinafter mL)) was added 20% ethanolic HCl (30 mL). The mixture was heated at reflux for about 20 hours (hereinafter h.), then allowed to cool. The solvent was removed in vacuo, and the residue was used without further purification.

Workup

  1. temperatureThe mixture was heated
  2. temperatureat reflux for about 20 hours (hereinafter h.)
  3. temperatureto cool
  4. customThe solvent was removed in vacuo
  5. customthe residue was used without further purification

Sources & evidence

ORD record
ord-adb8b398186444d59c917da1b4e15080
Source dataset
uspto-grants-1999_12
Patent number
US06008235

Reaction notes

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