Ethyl formate → HCID 17895307, compound
Reaction equation
[CH2:1]([C:8]1[CH:14]=[C:13]([Br:15])[CH:12]=[CH:11][C:9]=1[NH2:10])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH:16](OCC)=[O:17]>>[CH2:1]([C:8]1[CH:14]=[C:13]([Br:15])[CH:12]=[CH:11][C:9]=1[NH:10][CH:16]=[O:17])[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1Participants
3
Procedure
Using the general procedure of Coll. Czech. Chem. Commun. 1965, 30, 1163-1172, 2-benzyl-4-bromo-aniline, prepared as in Khim. Geterotsikl. Soedin. 1983, 3, 411-414, is heated with ethyl formate to afford the title compound.
Sources & evidence
- ORD record
- ord-ec0853d99ad34d2fae88e31438765cf8
- Source dataset
- uspto-grants-1999_12
- Patent number
- US06008213
Reaction notes
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