Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Diphenyl Ether | HCID 7583 | — |
| Reactant | Hexane | HCID 8058 | — |
| Reactant | HCID 19592399 | HCID 19592399 | — |
| Solvent | Biphenyl | HCID 7095 | — |
| Product | HCID 19592754 | HCID 19592754 | 84.1% |
Reaction Steps
A solution of 4-allyloxy-8-nitroquinoline (3.72 g) in biphenyl (2.59 g) and diphenyl ether (7.4 g) was heated at 200° C. for 10 minutes. After cooling, n-hexane (40 ml) was added thereto, and the mixture was warmed at 90° C. After cooling, the resulting precipitate was collected by filtration to give 3-allyl-1,4-dihydro-8-nitro-4-oxoquinoline (3.13 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06008230 |
|---|
| Source dataset | uspto-grants-1999_12 |
|---|
| ORD ID | ord-767e764fbfc34a279fda38e344f9c807 |
|---|
| Source note | uspto-grants-1999_12 |
|---|
